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1 article(s) from Battilocchio, Claudio

Integration of enabling methods for the automated flow preparation of piperazine-2-carboxamide

Richard J. Ingham,
Claudio Battilocchio,
Joel M. Hawkins and
Steven V. Ley

Beilstein J. Org. Chem. 2014, 10, 641–652, doi:10.3762/bjoc.10.56

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Graphical Abstract

Figure 1: Raspberry Pi^® (RPi) computer operating in the laboratory, shown here without its protective case. U...

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Figure 2: Two step approach to piperazine-2-carboxamide via hydrolysis followed by reduction. (a) Retrosynthe...

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Figure 3: Heterogeneous hydration of pyrazine-2-carbonitrile with hydrous zirconia.

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Figure 4: FlowIR™ profile for the reactor output after hydration of pyrazine-2-carbonitrile using hydrous zir...

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Figure 5: (a) Fluidic setup for the zirconia catalysed hydration of aromatic nitrile. (b) Raspberry Pi^® micro...

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Figure 6: Flowchart describing the control sequence for operating and monitoring the hydration reaction. The ...

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Figure 7: Profile for a 3 hour reaction simulating a long run. The absorbance shown is that at 1685 cm⁻¹, whi...

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Figure 8: Reactor setup for optimisation reactions. A multi-position valve (V2) was used for collecting sampl...

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Figure 9: Representation of the control sequence for running experiments under a set of conditions. (See Supporting Information File 3 for...

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Figure 10: Reduction products of piperazine-2-carboxamide.

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Figure 11: (a) In-line reservoir schematic. The liquid level is measured by observation of a plastic float. (b...

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Figure 12: Flow set up for the automated machine assisted synthesis of (R,S)-piperidine-2-carboxamide.

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Figure 13: Control sequence for the two-step process.

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Figure 14: Chart of monitored parameters over a 15 hour reaction. The output from the hydrolysis step is direc...

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Published 12 Mar 2014

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